2,6-Dimethylphenol → 22077-44-7

HRID 333664Notes

Reaction equation

HRID 333664 reaction equation
C[C:2]1[CH:7]=[CH:6][CH:5]=[C:4](C)[C:3]=1[OH:9].[P:10]([Cl:14])(Cl)(Cl)=[S:11].P(Cl)(Cl)(Cl)=O>>[P:10](=[S:11])([Cl:14])([O:9][C:3]1[CH:2]=[CH:7][CH:6]=[CH:5][CH:4]=1)[O:9][C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][CH:2]=1

Participants

4

Reactant 3

HCID 113352,6-DimethylphenolHCID 19883Thiophosphoryl chlorideHCID 24813Phosphorus oxychloride

Product 1

HCID 62513922077-44-7

Procedure

The title compound was prepared in similar fashion as compound 6, substituting phenol for 2,6-dimethylphenol and thiophosphoryl chloride for phosphorus oxychloride. The resulting oily residue was taken to the next step without further purification.

Workup

  1. customThe resulting oily residue was taken to the next step without further purification

Sources & evidence

ORD record
ord-1e4d25dca20949dbb07c2fa6c1bc08b2
Source dataset
uspto-grants-2014_11
Patent number
US08883765B2

Reaction notes

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