HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 86603969, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 86603970 | HCID 86603970 | — |
| Product | HCID 86603969 | HCID 86603969 | — |
Reaction Steps
5.00 g (13.8 mmol) tert-butyl [3-(2-amino-4-trifluoromethyl-phenylamino)-1,1-dimethyl-propyl]-carbamate and 6.73 g (41.5 mmol) 1,1′-carbonyldiimidazole are reacted and worked up analogously to method 2c). White solid. Yield: 4.18 g (78%); mass spectroscopy: [M−H]+=386.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07429583B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-7d4c92c665c74979b77007fc0d9312d3 |
| Source note | uspto-grants-2008_09 |