HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 334074Generated: October 29, 2026
Oxalyl chloride → HCID 86688296, compound
https://huagongshe.com/reaction/334074
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 6-Methoxypicolinic acid | HCID 570891 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86688296 | HCID 86688296 | — |
Reaction Steps
To a mixture of 5.00 g (32.7 mmol) 6-methoxy-pyridine-2-carboxylic acid in 100 mL DCM was added 40.8 mL (81.6 mmol) 2 M oxalyl chloride solution in DCM and stirred at 40° C. for 2 h. The solvent was removed by distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08883789B2 |
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| Source dataset | uspto-grants-2014_11 |
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| ORD ID | ord-7a3cb02637e540c3acfd20ff7e0b5407 |
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| Source note | uspto-grants-2014_11 |
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