HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86688293, compound → HCID 86688310, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86688293 | HCID 86688293 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86688310 | HCID 86688310 | — |
Reaction Steps
A mixture of 15 mg (31 μmol) [1-(3-chloro-phenyl)-1H-[1,2,4]-triazol-3-yl]-[4-(6-cyclopent-1-enyl-pyridine-2-carbonyl]-2,2-dimethyl-piperazin-1-yl]-methanone and 4 mg palladium on carbon in 5.0 mL EtOAc was hydrogenated at RT for 3.5 h. The catalyst was removed by filtration and the solvent was evaporated in vacuo. The resulting residue was purified by HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08883789B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-599e3fda95264e14b13669bee0c9ce52 |
| Source note | uspto-grants-2014_11 |