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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 334088Generated: October 30, 2026

HCID 86688293, compound → HCID 86688310, compound

https://huagongshe.com/reaction/334088

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86688293HCID 86688293—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 86688310HCID 86688310—

Reaction Steps

A mixture of 15 mg (31 μmol) [1-(3-chloro-phenyl)-1H-[1,2,4]-triazol-3-yl]-[4-(6-cyclopent-1-enyl-pyridine-2-carbonyl]-2,2-dimethyl-piperazin-1-yl]-methanone and 4 mg palladium on carbon in 5.0 mL EtOAc was hydrogenated at RT for 3.5 h. The catalyst was removed by filtration and the solvent was evaporated in vacuo. The resulting residue was purified by HPLC.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08883789B2
Source datasetuspto-grants-2014_11
ORD IDord-599e3fda95264e14b13669bee0c9ce52
Source noteuspto-grants-2014_11