HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Methoxyphenyl)piperazine → HCID 71602689, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Methoxyphenyl)piperazine | HCID 1346 | — |
| Reactant | 3'-Chloro[1,1'-biphenyl]-2-carbaldehyde | HCID 1392515 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | 1-(Biphenyl-2-ylmethyl)-4-phenylpiperazine | HCID 71602523 | — |
| Product | HCID 71602689 | HCID 71602689 | — |
Reaction Steps
250 mg of the target compound (0.64 mmol, 40.5%) was obtained using 1-(2-methoxyphenyl)piperazine (603 mg, 3.14 mmol), 3′-chlorobiphenyl-2-carbaldehyde (340 mg, 1.57 mmol) and NaBH(OAc)3 (1.0 g, 4.71 mmol) according to the synthesis method of Compound 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08883796B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-b144ba9174e5407891d369c7681886c2 |
| Source note | uspto-grants-2014_11 |