HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(p-Tolyl)piperazine → HCID 71678684, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(p-Tolyl)piperazine | HCID 83113 | — |
| Reactant | 3-Phenylbenzaldehyde | HCID 121053 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | 1-(Biphenyl-2-ylmethyl)-4-phenylpiperazine | HCID 71602523 | — |
| Product | HCID 71678684 | HCID 71678684 | — |
Reaction Steps
54.3 mg of the target compound (0.16 mmol, 36.4%) was obtained using 1-(4-methylphenyl)piperazine (154.8 mg, 0.88 mmol), biphenyl-3-carbaldehyde (80 mg, 0.44 mmol) and NaBH(OAc)3 (283.8 mg, 1.32 mmol) according to the synthesis method of Compound 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08883796B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-8e9ec2bca65b488db4450b75b1f5f896 |
| Source note | uspto-grants-2014_11 |