Phthalimide → HCID 66598006, compound

HRID 334715Notes

Reaction equation

HRID 334715 reaction equation
[CH3:1][Si:2]([CH3:9])([CH3:8])[C:3]#[C:4][CH2:5][CH2:6]O.[C:10]1(=[O:20])[NH:14][C:13](=[O:15])[C:12]2=[CH:16][CH:17]=[CH:18][CH:19]=[C:11]12>>[CH3:1][Si:2]([CH3:9])([CH3:8])[C:3]#[C:4][CH2:5][CH2:6][N:14]1[C:10](=[O:20])[C:11]2[C:12](=[CH:16][CH:17]=[CH:18][CH:19]=2)[C:13]1=[O:15]

Participants

3

Reactant 2

HCID 6809PhthalimideHCID 27608274-Trimethylsilyl-3-butyn-1-ol

Product 1

HCID 66598006HCID 66598006, compound

Procedure

The title compound was prepared in accordance with the general method of Example 109(D), from 4-(trimethylsilyl)but-3-yn-1-ol (3.20 g, 22.5 mmol) and phthalimide (3.50 g, 23.8 mmol).

Sources & evidence

ORD record
ord-8b4e1f83c0564391ac0b78771c75425a
Source dataset
uspto-grants-2014_11
Patent number
US08883826B2

Reaction notes

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