HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → N-benzyl-2-nitroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 1-Fluoro-2-nitrobenzene | HCID 73895 | — |
| Product | N-benzyl-2-nitroaniline | HCID 521800 | 93.3% |
Reaction Steps
The title compound was prepared in accordance with the general method of Example 195(A), from phenylmethanamine (3.51 g, 32.78 mmol) and 1-fluoro-2-nitrobenzene (4.40 g, 31.22 mmol). 6.65 g of N-benzyl-2-nitrobenzenamine (Yield: 93%) was obtained as an orange crystalline solid which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08883826B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-5d9faa7f04b04191a8f5694fb368be08 |
| Source note | uspto-grants-2014_11 |