HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-Amino-2-naphthol → HCID 178515717, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-Amino-2-naphthol | HCID 6865 | — |
| Edukt | HCID 178506061 | HCID 178506061 | — |
| Produkt | HCID 178515717 | HCID 178515717 | 57% |
Reaktionsschritte
The reaction of 7-bromo-2-chloro-5-(trifluoromethyl)-1H-benzo[d]imidazole (240 mg, 0.8 mmol, prepared according to the procedure described in WO 2004/035549 A1) with 5-amino-2-naphthol (64 mg, 0.4 mmol, TCI-US) under the condition of Example 2 afforded the title compound (57%) as an amorphous solid. MS (ESI, pos. ion) m/z: 423 (M+1).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07429608B2 |
| Quelldatensatz | uspto-grants-2008_09 |
| ORD ID | ord-c434a74d61304545bd72626243051fec |
| Quellennotiz | uspto-grants-2008_09 |