2-Bromobenzylamine → HCID 178471670, compound

HRID 336343Notes

Reaction equation

HRID 336343 reaction equation
[Br:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[CH2:4][NH2:5].CO[C:12](=[NH:20])[CH:13]([O:17][CH2:18][CH3:19])[O:14][CH2:15][CH3:16]>>[Br:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[CH2:4][NH:5][C:12](=[NH:20])[CH:13]([O:17][CH2:18][CH3:19])[O:14][CH2:15][CH3:16]

Participants

3

Reactant 2

HCID 3340722-BromobenzylamineHCID 17874536Methyl 2,2-diethoxyethanecarboximidate

Product 1

HCID 178471670HCID 178471670, compound

Procedure

Starting from 2-bromobenzylamine (20.00 g; commercial) and 2,2-diethoxy-ethanimidic acid methyl ester (24.46 g; 85% pure) and proceeding in analogy to Procedure A, the title compound was obtained as a yellow oil (39.31 g).

Sources & evidence

ORD record
ord-8db65d4f9a724acd9e9aaf645ffa4cc1
Source dataset
uspto-grants-2014_11
Patent number
US08889676B2

Reaction notes

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