HRID336367

反应详情

EQUATION

反应方程式

HRID 336367 的结构方程式

REACTANTS

反应物

2

结构：O=S(Cl)Cl

Thionyl chloride

Cl2OS

结构：Cc1cc(C(=O)O)ccc1Br

4-Bromo-3-methylbenzoic acid

C8H7BrO2

PRODUCTS

生成物

1

结构：Cc1cc(C(=O)Cl)ccc1Br

4-bromo-3-methylbenzoyl chloride

C8H6BrClO

收率 101.3%

PROCEDURE

实验过程

1 g 4-bromo-3-methyl-benzoic acid in 20 g thionylchloride was refluxed 1 h. The reaction was evaporated to give 1.1 g desired product.

WORKUP

后处理

customThe reaction was evaporated