HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Bromo-3-methylbenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-Bromo-3-methylbenzoic acid | HCID 82131 | — |
| Product | 4-Bromo-3-methylbenzoyl chloride | HCID 7021534 | 101.3% |
Reaction Steps
1 g 4-bromo-3-methyl-benzoic acid in 20 g thionylchloride was refluxed 1 h. The reaction was evaporated to give 1.1 g desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08889677B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-46323ba7c797469e8ef7cda78c5ef4b2 |
| Source note | uspto-grants-2014_11 |