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HRID336549

反应详情

EQUATION

反应方程式

HRID 336549 的结构方程式

REACTANTS

反应物

1
结构：CC(C)(C)OC(=O)N1CCC2(CC(N=[N+]=[N-])C2)C1
HCID86660640

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCC2(CC(N)C2)C1
HCID56962195

tert-Butyl 2-amino-6-azaspiro[3.4]octane-6-carboxylate

C12H22N2O2

收率 58.4%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)[O-].CC(=O)[O-].[Pb+2].[Pd]
催化剂HCID131709914

未命名化合物

PROCEDURE

实验过程

The process is performed according to the procedure described in Example 6 (step 6.4). Starting with 1.33 g (5.30 mmol) of tert-butyl 2-azido-6-azaspiro[3.4]octane-6-carboxylate (isomer 2′) and 0.54 g (2.65 mmol) of Lindlar catalyst (PdCaCO3), 0.70 g of product is obtained in the form of an oil.