HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 68765009, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 131732017 | HCID 131732017 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 68765009 | HCID 68765009 | 1,001.4% |
Reaction Steps
The process is performed according to the procedure described in Example 2 (step 2.5.). Starting with 0.86 g (2.13 mmol) of benzyl[6-(4-trifluoromethylpyrimidin-2-yl)-6-azaspiro[2.5]oct-1-yl]carbamate obtained in the preceding step and 3.74 mL (21.33 mmol) of a solution of 35% hydrobromic acid in acetic acid, and after basic extraction and uptake in diethyl ether, 0.32 g of product is obtained in the form of a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08889702B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-86b8264a808b44138f9fa6028bcf3043 |
| Source note | uspto-grants-2014_11 |