HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 60143703, compound → HCID 60143706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 60143703 | HCID 60143703 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 60143706 | HCID 60143706 | 40.6% |
Reaction Steps
86 mg of 2-(3,5-dimethyl-1H-pyrazol-1-yl)-5-nitrophenol was dissolved in 1.7 ml of ethanol, and 43 mg of 10% palladium/carbon was added and stirred under hydrogen atmosphere at room temperature for 45 minutes. After the insoluble matter was filtered off, the solvent was distilled off under reduced pressure to yield 30.4 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08889727B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-4aa6c05bcf6a49d8a81f22ed3d8ec902 |
| Source note | uspto-grants-2014_11 |