HRID337341

反应详情

EQUATION

反应方程式

HRID 337341 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

465 mg of 2-nitroresorcinol was dissolved in 9.3 ml of ethanol, and 230 mg of 10% palladium/carbon was added, and stirred under hydrogen atmosphere at room temperature for 1 hour. After the insoluble matter was filtered off, solvent was distilled off under reduced pressure to yield 338.5 mg of the title compound.

WORKUP

后处理

  1. filtrationAfter the insoluble matter was filtered off
  2. distillationsolvent was distilled off under reduced pressure