HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitroresorcinol → 2-Aminoresorcinol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitroresorcinol | HCID 11760 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Aminoresorcinol | HCID 69451 | 90.2% |
Reaction Steps
465 mg of 2-nitroresorcinol was dissolved in 9.3 ml of ethanol, and 230 mg of 10% palladium/carbon was added, and stirred under hydrogen atmosphere at room temperature for 1 hour. After the insoluble matter was filtered off, solvent was distilled off under reduced pressure to yield 338.5 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08889727B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-1261bf0bc10d482cb5c583bee02b0bae |
| Source note | uspto-grants-2014_11 |