HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86703257, compound → HCID 86703258, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86703257 | HCID 86703257 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86703258 | HCID 86703258 | 48.7% |
Reaction Steps
200 mg of 4-chloro-5-ethyl-2-nitrophenyl methanesulfonate was dissolved in 4 ml of ethanol, and 200 mg of 10% palladium/carbon was added and stirred under hydrogen atmosphere at room temperature for 4 hours. After the insoluble matter was filtered off, the solvent was distilled off under reduced pressure to yield 74.9 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08889727B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-d75ffef8555a48e083557ed81ab0eccc |
| Source note | uspto-grants-2014_11 |