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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 337829Generated: October 30, 2026

Hydrochloric Acid → HCID 89962578, compound

https://huagongshe.com/reaction/337829

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 89963338HCID 89963338—
SolventTetrahydrofuranHCID 8028—
ProductHCID 89962578HCID 8996257893.3%

Reaction Steps

The reaction and aftertreatment were conducted in the same manner as in Example 67c by using the 5-(9,9-dimethyl-1,4-dioxaspiro[4.5]dec-6-en-6-yl)-1-methyl-1H-pyrazole (758 mg, 3.05 mmol) prepared in Example 72b, 2 M hydrochloric acid (2.0 mL) and THF (5.0 mL), to yield the title compound (581 mg, 93%) as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08889741B2
Source datasetuspto-grants-2014_11
ORD IDord-1affef71a922431fa8aa9e3f1758d636
Source noteuspto-grants-2014_11