Hydrochloric Acid → 2-(3-Aminopyridazin-4-yl)cyclohex-2-en-1-one

Participants

Reaction Steps

The reaction and aftertreatment were conducted in the same manner as in Example 67c by using the crude 4-(1,4-dioxaspiro[4.5]dec-6-en-6-yl)pyridazin-3-amine prepared in Example 82c, 2 M hydrochloric acid (0.37 mL) and THF (0.92 mL), to yield the title compound (69 mg, 99%, 2 steps) as a colorless oil.

Provenance & Evidence