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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 337917Generated: October 30, 2026

Potassium Carbonate → HCID 89963531, compound

https://huagongshe.com/reaction/337917

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 89962738HCID 89962738—
SolventMethanolHCID 887—
ProductHCID 89963531HCID 89963531431.5%

Reaction Steps

The reaction and aftertreatment were conducted in the same manner as in Example 107e by using the (1S*,2R*)-3,3-difluoro-2-(1-methyl-1H-pyrazol-5-yl)cyclohexyl benzoate (206 mg, 0.643 mmol) prepared in Example 117c, potassium carbonate (270 mg, 1.95 mmol) and methanol (4.0 mL), to yield the title compound (600 mg, 43%) as a colorless solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08889741B2
Source datasetuspto-grants-2014_11
ORD IDord-4c3a47be454e45f79a433d2c8f92c3ba
Source noteuspto-grants-2014_11