HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 89963531, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 89962738 | HCID 89962738 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 89963531 | HCID 89963531 | 431.5% |
Reaction Steps
The reaction and aftertreatment were conducted in the same manner as in Example 107e by using the (1S*,2R*)-3,3-difluoro-2-(1-methyl-1H-pyrazol-5-yl)cyclohexyl benzoate (206 mg, 0.643 mmol) prepared in Example 117c, potassium carbonate (270 mg, 1.95 mmol) and methanol (4.0 mL), to yield the title compound (600 mg, 43%) as a colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08889741B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-4c3a47be454e45f79a433d2c8f92c3ba |
| Source note | uspto-grants-2014_11 |