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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 337933Generated: October 29, 2026

HCID 89962762, compound → HCID 89962427, compound

https://huagongshe.com/reaction/337933

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 89962762HCID 89962762—
CatalystNickelHCID 935—
SolventIsopropanolHCID 3776—
ProductHCID 89962427HCID 8996242728.5%

Reaction Steps

The reaction and aftertreatment were conducted in the same manner as in Example 102c by using the 1-methyl-5-[(1S,6S)-7-oxabicyclo[4.1.0]hept-1-yl]-1H-pyrazole (0.21 g, 1.17 mmol) prepared in Example 123d, Raney nickel (2.0 g) and isopropanol (5.9 mL), to yield the title compound (0.060 g, 28%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08889741B2
Source datasetuspto-grants-2014_11
ORD IDord-65a59f5547634cde8090e7c4a6321419
Source noteuspto-grants-2014_11