HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 89963376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 89962299 | HCID 89962299 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 89963376 | HCID 89963376 | 100.1% |
Reaction Steps
The reaction and aftertreatment were conducted in the same manner as in Example 107e by using the (1S*,2R*)-4,4-difluoro-2-{1-[(2-methoxyethoxy)methyl]-1H-pyrazol-5-yl}cyclohexyl benzoate (547 mg, 1.39 mmol) prepared in Example 157b, potassium carbonate (19 mg, 0.139 mmol) and methanol (10 mL), to yield the title compound (404 mg, 99%) as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08889741B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-585de214735d4668991c238c457ff622 |
| Source note | uspto-grants-2014_11 |