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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 337992Generated: October 28, 2026

Potassium Carbonate → HCID 89963376, compound

https://huagongshe.com/reaction/337992

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 89962299HCID 89962299—
SolventMethanolHCID 887—
ProductHCID 89963376HCID 89963376100.1%

Reaction Steps

The reaction and aftertreatment were conducted in the same manner as in Example 107e by using the (1S*,2R*)-4,4-difluoro-2-{1-[(2-methoxyethoxy)methyl]-1H-pyrazol-5-yl}cyclohexyl benzoate (547 mg, 1.39 mmol) prepared in Example 157b, potassium carbonate (19 mg, 0.139 mmol) and methanol (10 mL), to yield the title compound (404 mg, 99%) as a yellow oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08889741B2
Source datasetuspto-grants-2014_11
ORD IDord-585de214735d4668991c238c457ff622
Source noteuspto-grants-2014_11