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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 338016Generated: October 29, 2026

Potassium Carbonate → HCID 89962701, compound

https://huagongshe.com/reaction/338016

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 89962785HCID 89962785—
SolventMethanolHCID 887—
ProductHCID 89962701HCID 8996270187%

Reaction Steps

The reaction and aftertreatment were conducted in the same manner as in Example 162f by using the (1S*,2R*,5S*)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-(1-methyl-1H-pyrazol-5-yl)cyclohexyl benzoate (327 mg, 1.09 mmol) prepared in Example 163e, potassium carbonate (301 mg, 2.18 mmol) and methanol (5.0 mL), to yield the title compound (207 mg, 87%) as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08889741B2
Source datasetuspto-grants-2014_11
ORD IDord-7bbdbd7ba4be487f95fcd06c04426505
Source noteuspto-grants-2014_11