HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 89962701, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 89962785 | HCID 89962785 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 89962701 | HCID 89962701 | 87% |
Reaction Steps
The reaction and aftertreatment were conducted in the same manner as in Example 162f by using the (1S*,2R*,5S*)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-(1-methyl-1H-pyrazol-5-yl)cyclohexyl benzoate (327 mg, 1.09 mmol) prepared in Example 163e, potassium carbonate (301 mg, 2.18 mmol) and methanol (5.0 mL), to yield the title compound (207 mg, 87%) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08889741B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-7bbdbd7ba4be487f95fcd06c04426505 |
| Source note | uspto-grants-2014_11 |