HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 89962245, compound → HCID 89962729, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 89962245 | HCID 89962245 | — |
| Solvent | Isopropanol hexane | HCID 21585144 | — |
| Product | HCID 89962729 | HCID 89962729 | — |
Reaction Steps
The (1S*,2R*,4R*)-4-{[tert-butyl(dimethyl)silyl]oxy}-2-(1-methyl-1H-pyrazol-5-yl)cyclohexanol prepared in Example 161a was optically resolved with CHIRALFLASH IC (Daicel Corp.; hexane/isopropanol=6:4) to yield the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08889741B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-16cd94aa1b8c4e64a113263ae7e1581e |
| Source note | uspto-grants-2014_11 |