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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 338030Generated: October 29, 2026

HCID 89962754, compound → HCID 89962599, compound

https://huagongshe.com/reaction/338030

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 89962754HCID 89962754—
CatalystHCID 178418390HCID 178418390—
SolventTetrahydrofuranHCID 8028—
ProductHCID 89962599HCID 8996259922%

Reaction Steps

The reaction and aftertreatment were conducted in the same manner as in Example 167b by using the (3aR,7aR)-3a-(1-methyl-1H-pyrazol-5-yl)hexahydro-1,3-benzodioxol-2-one (760 mg, 3.42 mmol) prepared in Example 168b, palladium carbon (10%; 760 mg) and THF (10 mL), to yield the title compound (133 mg, 22%) as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08889741B2
Source datasetuspto-grants-2014_11
ORD IDord-1b64a42225f64bfc8b8acfc63577d1f1
Source noteuspto-grants-2014_11