HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminothiophenol → 2-(4-(Benzo[d]thiazol-2-yl)phenoxy)-2-methylpropanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminothiophenol | HCID 8713 | — |
| Reactant | Ethyl 2-(4-formylphenoxy)-2-methylpropanoic acid | HCID 86709921 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-(4-(Benzo[d]thiazol-2-yl)phenoxy)-2-methylpropanoic acid | HCID 60194687 | — |
Reaction Steps
In a methanol solvent, a solution including Compound 97c (1.0 eq.) and 2-aminothiophenol (1.0 eq.) was stirred at room temperature. After methanol was removed, the precipitate was filtered, and washed with cold methanol to obtain a solid target product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08889881B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-c8091baed8be4d3a89607f90b517ec91 |
| Source note | uspto-grants-2014_11 |