HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aspirin → HCID 66976703, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aspirin | HCID 2244 | — |
| Reactant | (-)-Carnitine | HCID 10917 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66976703 | HCID 66976703 | — |
Reaction Steps
L-Carnitine (1.61 g, 10 mmol) and acetylsalicylic acid (1.80 g, 10 mmol) were dissolved in ethanol (20 ml) and the solution concentrated in vacuo at about 40° C. till syrup consistence that on cooling crystallizes. The crystalline mass was triturated with acetone (50 ml), filtered, washed with acetone and dried in vacuo at room temperature. The yield of colorless crystals with m.p. 90-94° C. was 3.17 g (93%). The substance is water soluble, stable at ambient conditions.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08889902B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-94f0c49345d046b6b7eff6d24ae1e96d |
| Source note | uspto-grants-2014_11 |