Stannous chloride dihydrate → HCID 67236560, compound

Participants

Reaction Steps

Prepared as described in the Nitro Reduction section using 2-(4-nitro-2-trifluoromethylphenyl)-6-methoxybenzothiazole (0.6 g, 1.69 mmol) and tin (II) dichloride dihydrate (3.06 g, 13.56 mmol) in EtOH (35 ml) to give the title compound (0.51 g, 93%) as a colourless solid after work-up and flash chromatography (30:1 DCM/EtOAc).

Provenance & Evidence