HRID339503

反应详情

EQUATION

反应方程式

HRID 339503 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Prepared as described in the Nitro Reduction section using 2-(2-methoxy-4-nitrophenyl)-6-methoxybenzothiazole (1.0 g, 3.13 mmol) and tin (II) dichloride dihydrate (5.66 g, 25.08 mmol) in EtOH (50 ml) to give the title compound (0.79 g, 89%) as a pale yellow solid after work-up and recrystallisation from EtOH.

WORKUP

后处理

  1. customPrepared