HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Hydrazinopyridine → HCID 67233679, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Hydrazinopyridine | HCID 78645 | — |
| Reactant | HCID 86654355 | HCID 86654355 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67233679 | HCID 67233679 | 80.9% |
Reaction Steps
To the product from Step C (2.95 g, 8.05 mmol) was added EtOH (30 mL, anhydrous). To this solution was added 2-hydrazinylpyridine (0.967 g, 8.86 mmol). The mixture was stirred at ambient temperature for 24 hours. The resulting precipitate was isolated by vacuum filtration and washed with cold EtOH and then dried in vacuo to afford 2.98 g (73%) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895550B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-02e6e734ea0440f2845aa63c37550da8 |
| Source note | uspto-grants-2014_11 |