HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 57384593, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 57384852 | HCID 57384852 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57384593 | HCID 57384593 | — |
Reaction Steps
The product from step (iii) (0.39 g) was dissolved in DCM (20 mL) and triethylamine (0.15 g) added, followed by addition of methanesulfonyl chloride (0.3 mL) and the mixture stirred for 5 hrs. The mixture was concentrated in vacuo to afford the subtitle compound as a crude product (0.45 g); MS multimode (+) 579.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895570B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-a788f95360d54e969d199d1224bcdbcb |
| Source note | uspto-grants-2014_11 |