HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 58213655, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 86652358 | HCID 86652358 | — |
| Product | HCID 58213655 | HCID 58213655 | — |
Reaction Steps
4-(2-(5-Amino-8-methylbenzo[f][1,7]naphthyridin-2-yl)ethyl)-3-methylbenzamide was prepared from 4-(2-(5-amino-8-methylbenzo[f][1,7]naphthyridin-2-yl)ethyl)-3-methylbenzoyl chloride (Example 116/Step 2) and ammonia following the procedures described for Example 117. 1H NMR (CDCl3): δ 8.60 (s, 1H), 8.35 (s, 1H), 8.05 (d, 1H), 7.65 (s, 1H), 7.51-7.53 (m, 2H), 7.13-7.21 (m, 2H), 3.09-3.16 (m, 4H), 2.51 (s, 3H), 2.34 (s, 3H). LRMS [M+H]=371.2
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895577B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-6efbd7566e9649989797426fad1ffe84 |
| Source note | uspto-grants-2014_11 |