4-Methoxybenzylamine → HCID 59771204, compound

HRID 340579Notes

Reaction equation

[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([CH:10]2[CH2:15][S:14](=[O:17])(=[O:16])O[S:12](=[O:19])(=[O:18])[CH2:11]2)=[CH:6][CH:5]=1)([O-:3])=[O:2].[CH3:20][O:21][C:22]1[CH:29]=[CH:28][C:25]([CH2:26][NH2:27])=[CH:24][CH:23]=1>>[CH3:20][O:21][C:22]1[CH:29]=[CH:28][C:25]([CH2:26][N:27]2[S:12](=[O:18])(=[O:19])[CH2:11][CH:10]([C:7]3[CH:6]=[CH:5][C:4]([N+:1]([O-:3])=[O:2])=[CH:9][CH:8]=3)[CH2:15][S:14]2(=[O:16])=[O:17])=[CH:24][CH:23]=1

Participants

Reactant 2

HCID 754524-Methoxybenzylamine

HCID 59771193HCID 59771193, compound

Product 1

HCID 59771204HCID 59771204, compound

Procedure

A solution of 4-(4-nitro-phenyl)-[1,2,6]oxadithiane 2,2,6,6-tetraoxide (as prepared in the previous step) is treated with 4-methoxy-benzylamine according to the procedure of Example 2, step (c) to afford the title compound.

Sources & evidence

ORD record: ord-50ae16f33678461888a12f6bacd5ad32
Source dataset: uspto-grants-2014_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08895584B2

Reaction notes

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