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HRID340878

反应详情

EQUATION

反应方程式

HRID 340878 的结构方程式

REACTANTS

反应物

2
结构：N
HCID222

Ammonia gas

H3N

结构：CC(=O)Oc1cc(C(=O)Cl)cc(C(=O)Cl)c1.CC(O)/C=C/C(C)O
HCID131732095

未命名化合物

PRODUCTS

生成物

1
结构：CC(O)/C=C/C(C)O.O=C(Cl)c1cc(O)cc(C(=O)Cl)c1
HCID131732096

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

To a solution of methanolic ammonia (20 mL, 1 N), polymer (126) dissolved in 5 mL tetrahydrofuran is added and the solution is stirred for two hours. The polymer was then precipitated in 100 mL of cold 1 N hydrochloric acid and collected by filtration. The polymer was then dried under high vacuum and was found to have a molecular weight of ˜5,000 g/mol by GPC.

WORKUP

后处理

  1. additionis added
  2. customThe polymer was then precipitated in 100 mL of cold 1 N hydrochloric acid
  3. filtrationcollected by filtration
  4. customThe polymer was then dried under high vacuum