HuagongsheHuagongshe Chemistry Print Report · For research reference only
(5-Azidomethyl-furan-2-ylmethyl)-carbamic Acid Tert-Butyl Ester → HCID 60035026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (5-Azidomethyl-furan-2-ylmethyl)-carbamic Acid Tert-Butyl Ester | HCID 60053847 | — |
| Catalyst | Lindlars catalyst | HCID 131709914 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 60035026 | HCID 60035026 | 101.9% |
Reaction Steps
To a solution of 88.6 mg of (5-azidomethyl-furan-2-ylmethyl)-carbamic acid tert-butyl ester in 3 mL of ethanol was added 30 mg of Lindlar catalyst, stirred at room temperature under hydrogen atmosphere for 15 hours, the catalyst filtered off, and the solvent was evaporated, to afford 81 mg of the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07429609B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-c1cd73bbdc5141dab72dbd3f5b96d8e6 |
| Source note | uspto-grants-2008_09 |