HRID341166

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID9773

Ethanamine, 2,2,2-trifluoro-

C2H4F3N

结构：CC1(C)OB(c2cccc(NC(=O)NCC(F)(F)F)c2)OC1(C)C

HCID57497691

N-[3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-N′-(2,2,2-trifluoroethyl)urea

C15H20BF3N2O3

PRODUCTS

生成物

结构：CNC(=O)Nc1cccc(B2OC(C)(C)C(C)(C)O2)c1

HCID10802372

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

Prepared as described for 1-[3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-3-(2,2,2-trifluoro-ethyl)-urea (I6), substituting methylamine in THF (2M) for 2,2,2-trifluoroethyl amine in Step 1. 1H NMR (400 MHz, CDCl3): 7.59-7.53 (2H, m), 7.50 (1H, d), 7.34 (1H, t), 2.83 (3H, s), 1.33 (12H, s).

WORKUP

后处理

customPrepared