Methyl isothiocyanate → HCID 59320877, compound

Participants

Reaction Steps

A mixture of 1-[3-(7-hydrazinocarbonyl-imidazo[1,2-a]pyridin-3-yl)-phenyl]-3-(2,2,2-trifluoro-ethyl)-urea (90 mg, 0.23 mmol) and methyl isothiocyanate (17 mg, 0.23 mmol) were heated in EtOH (3 ml) at 70° C. for 18 h. The reaction mixture was allowed to cool and the precipitate formed filtered off to give the product (34 mg). MS: [M+H]+ 447

Provenance & Evidence