HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86709904, compound → HCID 70673852, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86709904 | HCID 86709904 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Product | HCID 70673852 | HCID 70673852 | 48.4% |
Reaction Steps
4-(1-Methyl-1-silacyclopentan-1-yl)-3-cyanobutanoic acid (555 mg, 2.63 mmol) was subjected to catalytic reduction in the presence of Pd(OH)2 in the same manner as that of Example 20, the solvent was evaporated, and the residue was recrystallized to obtain 4-amino-3-[(1-methyl-1-silacyclopentan-1-yl)methyl]butanoic acid (274 mg, 48%) mentioned in the title as colorless powdery crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895769B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-d7348cbe4d794038979572ebcd2c6ec9 |
| Source note | uspto-grants-2014_11 |