HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → DL-beta-Phenylalanine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Malonic Acid | HCID 867 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | DL-beta-Phenylalanine | HCID 69189 | — |
Reaction Steps
A suspension of 100 g of benzaldehyde, 94 g of malonic acid, 109 g of ammonium acetate in 300 cm3 of ethanol, is brought to boiling point in a nitrogen atmosphere, under vigorous stirring. The suspension is mantained under the above conditions for about eight hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05856311 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-66fb23c058584097a0d7ac31bac82c6e |
| Source note | uspto-grants-1999_01 |