huagongshe.com
HRID34196

反应详情

EQUATION

反应方程式

HRID 34196 的结构方程式

REACTANTS

反应物

4
结构：CCN(C(C)C)C(C)C
HCID81531

Diisopropylethylamine

C8H19N

结构：O=C1CNCCN1
HCID231360

Piperazin-2-one

C4H8N2O

结构：CN(C)C(Oc1c(F)c(F)c(F)c(F)c1F)=[N+](C)C.F[P-](F)(F)(F)(F)F
HCID15840204

(Dimethylamino)-N,N-dimethyl(pentafluorophenoxy)methaniminium hexafluorophosphate

C11H12F11N2OP

结构：CC(Nc1ncnc2cc(C(=O)O)c(Cl)cc12)c1nc2cc(Cl)ccc2[nH]1
HCID178463504

未命名化合物

PRODUCTS

生成物

1
结构：CC(Nc1ncnc2cc(C(=O)N3CCNC(=O)C3)c(Cl)cc12)c1nc2cc(Cl)ccc2[nH]1
HCID178463498

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

PROCEDURE

实验过程

Prepared analogously to Example 37a from 6-chloro-4-[1-(5-chloro-1H-benzimidazol-2-yl)-ethylamino]-7-hydroxycarbonyl-quinazoline, pentafluorophenyl-tetramethyluronium-hexafluorophosphate (PFTU), diisopropylethylamine and piperazinone in DMSO at ambient temperature.