HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 17933657, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 22133000 | HCID 22133000 | — |
| Reactant | HCID 178418443 | HCID 178418443 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 17933657 | HCID 17933657 | — |
Reaction Steps
The operation is carried out as in Stage 2 of Example 1 starting with 6 g of the product obtained in Stage 1 of Example 1 in 300 ml of a methylene chloride/sulphuric ether mixture (60/240), to which 4.6 ml of ethyl magnesium bromide is added dropwise, then the whole is maintained under agitation for 30 minutes at ambient temperature and then 100 ml of ice-cooled water is introduced into the reaction medium obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05856509 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-461b754bf2cb4a41b75ae6d1bc7e0f9e |
| Source note | uspto-grants-1999_01 |