HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 54278802, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | HCID 54108474 | HCID 54108474 | — |
| Catalyst | Manganese oxide | HCID 160959 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 54278802 | HCID 54278802 | — |
Reaction Steps
The operation is carried out as in Example 9 starting with 2 g of the product of Example 20 using 10 g of manganese oxide, 1 g of sodium cyanide, 200 ml of methanol, 40 ml of methylene chloride and 600 ul of acetic acid, in this way 1.64 g of expected product is obtained (M.p.=161° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05856509 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-3f577259a7a748b98a15d36aa6b42723 |
| Source note | uspto-grants-1999_01 |