Hydrochloric Acid → HCID 22941049, compound

Participants

Reaction Conditions

Reaction Steps

The product from Step D was dissolved in ethyl acetate, cooled to -40° C. under nitrogen, and the solution saturated with HCl(g). The solution was warmed to 0° C. for 30 min, and then purged with nitrogen. The solvent was removed in vacuo. The product was evaporated from ethyl acetate three times. The title compound was obtained as a white solid.

Provenance & Evidence