HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 4-(2-(4-n-Propylphenyl)ethyl)cyclohexanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 4-(2-(4-n-Propylphenyl)ethenyl)cyclohexanone | HCID 53917570 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | HCID 178418361 | HCID 178418361 | — |
| Product | 4-(2-(4-n-Propylphenyl)ethyl)cyclohexanone | HCID 54333138 | 94% |
Reaction Steps
In a liquid mixture comprising 200 ml of ethanol and 200 ml of toluene was dissolved 42 g of the 4-(2-(4-n-propylphenyl)ethenyl)cyclohexanone mentioned above, 4 g of palladium/carbon (5%) was added as catalyst, and they were subjected to a catalytic reduction in hydrogen gas atmosphere. After finishing of the reaction, the catalyst was filtered off and the solvent was distilled off under a reduced pressure to obtain 39.8 g of 4-(2-(4-n-propylphenyl)ethyl)cyclohexanone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05858275 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-174de323b7bc4164978b4d180f1e51cc |
| Source note | uspto-grants-1999_01 |