HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiourea → HCID 86753554, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | HCID 86753556 | HCID 86753556 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86753554 | HCID 86753554 | 91.6% |
Reaction Steps
A mixture of 3-chloroacetyl-2-methyl-7-nitrobenzo[b]furan (431 mg) and thiourea (194 mg) in ethanol (10 ml) was refluxed for 1.5 hours. The separated solid was collected, washed with ethanol and dried to give 3-(2-aminothiazol-4-yl)-2-methyl-7-nitrobenzo[b]furan hydrochloride (485 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05858995 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-0fdc73e4992444149414c304b86cbdc8 |
| Source note | uspto-grants-1999_01 |