HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70196728, compound → HCID 70200722, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70196728 | HCID 70196728 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 70200722 | HCID 70200722 | 88.4% |
Reaction Steps
A solution of 7-[2,6-dichloro-3-(2-methoxyethyl)oxymethoxymethylbenzoylamino]-2,3-dimethylbenzo[b]furan (305 mg) in 10% methanolic hydrogen chloride (4.5 m.l) was refluxed for 1 hour. The reaction mixture was cooled and the separated solid was collected to give 7-(2,6-dichloro-3-hydroxymethylbenzoylamino)-2,3-dimethylbenzo[b]furan (217 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05858995 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-e9301500c12e49afbb5c3cd1998e4255 |
| Source note | uspto-grants-1999_01 |