HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Chlorophenyl)-2-piperazinone → HCID 54004906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Chlorophenyl)-2-piperazinone | HCID 15400016 | — |
| Reactant | HCID 53849539 | HCID 53849539 | — |
| Product | HCID 54004906 | HCID 54004906 | — |
Reaction Steps
The product of step B is heated with 1-(2-chlorophenyl)-piperazin-2-one (1 molar equivalent). The crude N-oxide of 4-[3-(4-methoxybenzyl)pyrid -4-yl]-I-(2-chlorophenyl)-piperazin-2-one is deoxygenated by treatment with triphenylphosphine (2 molar equivalents) to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05859015 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-0b4e27cadee940f98cdaf1acf8608f73 |
| Source note | uspto-grants-1999_01 |