HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 4-Acetylbenzenesulphonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 4-Acetylbenzenesulfonyl chloride | HCID 266418 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-Acetylbenzenesulphonamide | HCID 74065 | — |
Reaction Steps
131 g of product of Example 3 are added portionwise to 1 l of ethanol saturated with ammonia. The reaction mixture is stirred at ambient temperature for 24 h, then concentrated and water is added thereto. The solid obtained is filtered, then washed with isopropanol and pentane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05859036 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-c6e9ade2c5f14ec1a34bc4390c80e5d0 |
| Source note | uspto-grants-1999_01 |