HCID 10960386, compound → HCID 10981846, compound

HRID 342654Notes

Reaction equation

HRID 342654 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([N:8]2[C:12]([C:14]3[CH:19]=[CH:18][C:17]([S:20]([NH2:23])(=[O:22])=[O:21])=[CH:16][CH:15]=3)(O)[CH2:11][S:10][C:9]2=[S:24])[CH:5]=[CH:6][CH:7]=1>C(O)C.Cl>[Cl:1][C:2]1[CH:3]=[C:4]([N:8]2[C:12]([C:14]3[CH:15]=[CH:16][C:17]([S:20]([NH2:23])(=[O:21])=[O:22])=[CH:18][CH:19]=3)=[CH:11][S:10][C:9]2=[S:24])[CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 1

HCID 10960386HCID 10960386, compound

Product 1

HCID 10981846HCID 10981846, compound

Reagents, catalysts & solvents 2

HCID 313Hydrochloric AcidSolventHCID 702EthanolSolvent

Procedure

5.4 g of the product of Example 7 are dissolved in 50 ml of ethanol to which 1 ml of concentrated hydrochloric acid has been added. The reaction mixture is refluxed for 1 h, then filtered. The solid obtained is washed with ethanol, then with pentane.

Workup

  1. additionhas been added
  2. temperatureThe reaction mixture is refluxed for 1 h
  3. filtrationfiltered
  4. customThe solid obtained
  5. washis washed with ethanol

Sources & evidence

ORD record
ord-eb0ec4bc265a47e18acb1dafa51545c9
Source dataset
uspto-grants-1999_01
Patent number
US05859036

Reaction notes

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